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Current Status of ISO/TC202 – Microbeam Analysis

This note is to provide the status of the ISO Committee in charge of Microbeam Analysis standards. It will cover the general organizational structure of the committee, current standards, proposed standards, and member contributions.

Patrick Camus1, Douglas Meier2, and Ryna Marienko3

1EDAX Inc., 91 McKee Place, Mahwah, NJ 07430

2McCrone Associates, Inc., 850 Pasquinelli Drive, Westmont, IL 60559

3NIST; MS 8371, 100 Bureau Dr., Gaithersburg, MD 20899

 

 

 

 “We're ISO, the International Organization for Standardization. We develop and publish International Standards.”

 

This note is to provide the status of the ISO Committee in charge of Microbeam Analysis standards. It will cover the general organizational structure of the committee, current standards, proposed standards, and member contributions.

The authors are the US representatives to the Technical Committee for Microbeam Analysis, TC202. It also maintains 4 sub-committees (SC) on specific topics: Terminology, Electron probe microanalysis, Analytical electron microscopy, and Scanning electron microscopy. The scope of its work is standardization in the field of microbeam analysis (measurement, parameters, methods and reference materials) which uses electrons as an incident beam and electrons and photons as the detection signal; the purpose is to analyze the compositional and structural characteristics of solid materials; the volume of analysis will generally involve a depth up to 10 micrometers and a surface area less than 100 square micrometers.

The members of TC202 do not work totally independently but have collaborations with other committees whose interests parallel theirs. These committees include TC24 – Particle Characterization, TC201 – Surface Chemical Analysis, and TC229 – Nanotechnologies.

There are a number of Contributing Nations and Sponsoring Organizations that have active membership in TC202: China (SAC), Germany (DIN), Iran, Islamic Republic of (ISIRI), Japan (JISC), Korea, Republic of (KATS), Netherlands (NEN), Russian Federation (GOST R), Sweden (SIS), Uganda (UNBS), United Kingdom (BSI), and United States (ANSI)

There are currently 18 international standards published by ISO on the topic of Microbeam Analysis.

Reference

Document title

ISO 13067:2011

Electron backscatter diffraction -- Measurement of average grain size

ISO 15632:2012

Selected instrumental performance parameters for the specification and checking of energy-dispersive X-ray spectrometers for use in electron probe microanalysis

ISO 22029:2012

EMSA/MAS standard file format for spectral-data exchange

ISO 22309:2011

Quantitative analysis using energy-dispersive spectrometry (EDS) for elements with an atomic number of 11 (Na) or above

ISO 24173:2009

Guidelines for orientation measurement using electron backscatter diffraction

ISO 15932:2013

Analytical electron microscopy – Vocabulary *

ISO 22493:2014

Scanning electron microscopy – Vocabulary *

ISO 23833:2013

Electron probe microanalysis (EPMA) -- Vocabulary *

ISO 11938:2012

Methods for elemental-mapping analysis using wavelength-dispersive spectroscopy

ISO 14594:2014

Guidelines for the determination of experimental parameters for wavelength dispersive spectroscopy

ISO 14595:2014

Guidelines for the specification of certified reference materials (CRMs)

ISO 16592:2012

Guidelines for determining the carbon content of steels using a calibration curve method

ISO 17470:2014

Guidelines for qualitative point analysis by wavelength dispersive X-ray spectrometry

ISO 22489:2016

Quantitative point analysis for bulk specimens using wavelength dispersive X-ray spectroscopy

ISO 25498:2010

Selected-area electron diffraction analysis using a transmission electron microscope

ISO 29301:2010

Methods for calibrating image magnification by using reference materials having periodic structures

ISO 16700:2016

Guidelines for calibrating image magnification

ISO/TS 24597:2011

Methods of evaluating image sharpness

There are several proposals that are being evaluated that are Work-in-Progress

Reference

Document title

ISO/WD 20720

Methods of the specimen preparation for particle analysis

ISO/NP 22079

Electron Backscattered Electron Diffraction -- Vocabulary *

ISO/DIS 19463

Guidelines for performing quality assurance procedures

ISO/DIS 20263

Determination method for interface position in the cross-sectional image of the layered materials

ISO/DIS 25498

Selected-area electron diffraction analysis using a transmission electron microscope

ISO/DIS 29301

Methods for calibrating image magnification by using reference materials having periodic structures

ISO/FDIS 19214

Guidelines for apparent growth direction determination of wirelike crystals by transmission electron microscopy

ISO/AWI 21466

Method for evaluating critical dimensions by CD-SEM

 

ISO/AWI TS 21383

Qualification of the scanning electron microscope for quantitative measurements

 

ISO/CD 20171

Tag image file format for Scanning electron microscopy (TIFF/SEM)

 

The ISO vocabulary documents and terms for all TC can be freely searched on the ISO website at:
                https://www.iso.org/obp/ui/#search

Volunteers are need from each of the participating member nations for TC202 to accomplish its goals. Some of the tasks that they perform are:

•       Strive to create standards which will benefit users in selecting or using microbeam instruments.

•       Make decisions on proposals and renewals for standards,

•       Offer technical and editorial input on draft standards,

•       Attendance at an annual meeting at an international location.

•       Submit proposals

•       Act as national member body experts during the review of proposals and renewals.

Some of you may be asking yourself “Why should I participate?”

•       To use your expertise to improve the work of others in the field by standardizing the operating procedures and reference materials.

•       To create standard procedures to increase the quality of operators’ work, increasing the stature of the technique and the reputation of everyone in the field.

•       To develop standard specifications and standard methods that benefit instrument operators and consumers of microanalytical data and analysis

•       To encourage manufacturers to adopt higher quality and meaningful specifications

•       To encourage industry to implement consistent testing and reporting

A reader can become involved in ISO TC202 by contacting your national member body representative.

We look forward to your participation

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